Difference between revisions of "Agitated Dryers"
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[[Category:Drying]]{{Knoppen}} | [[Category:Drying]]{{Knoppen}} | ||
[[File:Agitated_Dryers.jpg|200px|right|thumb|Agitated Dryers]] | |||
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The '''Agitated Dryers''' are presently used widely over the chemical Industry. These are naturally of 2 different types. These are: | The '''Agitated Dryers''' are presently used widely over the chemical Industry. These are naturally of 2 different types. These are: | ||
# Agitated Thin Film Dryers | # Agitated Thin Film Dryers | ||
# Agitated Vacuum Dryers | # Agitated Vacuum Dryers | ||
==Agitated Thin Film Dryers== | ==Agitated Thin Film Dryers== | ||
Mechanically Agitated Thin Film Dryer is an indirectly heated continuous dryer. The feed can be in the form of a solution, slurry, wet cake or paste. If required it operates under vacuum. We offer both vertical and horizontal versions. Mechanically Agitated Thin Film Dryer is an indirectly heated continuous dryer. The feed can be in the form of a solution, slurry, wet cake or paste. If required it operates under vacuum. We offer both vertical and horizontal versions. | Mechanically Agitated Thin Film Dryer is an indirectly heated continuous dryer. The feed can be in the form of a solution, slurry, wet cake or paste. If required it operates under vacuum. We offer both vertical and horizontal versions. Mechanically Agitated Thin Film Dryer is an indirectly heated continuous dryer. The feed can be in the form of a solution, slurry, wet cake or paste. If required it operates under vacuum. We offer both vertical and horizontal versions. | ||
==Working Principle== | |||
The drying in a agitated thin film dryer is a continuous operation under vacuum. Operating pressures can be as low as 1 mbar and operating temperatures can be as high as 350oC. Drying time depends on material being dried, amount of solvent to be removed, desired final moisture content, permissible jacket temperature etc.The vertical Agitated Thin Film Dryer has a jacketed cylinder with a closely fitting rotor at the centre. During operation the rotor revolves at high speed. The feed distributor spreads the incoming feed uniformly over the cylinder top periphery. The rotor blades pick up the material, spread it over heated surface in a thin film and agitate the film intensely, as it rapidly travels down. The material transforms from solution to slurry, wet cake, wet powder and finally dry powder as it travels from top to bottom. The vapour generated rises counter-currently to the inbuilt entrainment separator. Here the entrained droplets are separated from the vapour stream. The clean vapour leaves the dryer through the vapour nozzle at top.The horizontal version of the dryer is used for drying of wet cake, pastes, wet powders. The wet feed enters at one end and dry powder leaves from the opposite end. The vapours move counter currently to the powder flow and leave through vapour nozzle. | The drying in a agitated thin film dryer is a continuous operation under vacuum. Operating pressures can be as low as 1 mbar and operating temperatures can be as high as 350oC. Drying time depends on material being dried, amount of solvent to be removed, desired final moisture content, permissible jacket temperature etc.The vertical Agitated Thin Film Dryer has a jacketed cylinder with a closely fitting rotor at the centre. During operation the rotor revolves at high speed. The feed distributor spreads the incoming feed uniformly over the cylinder top periphery. The rotor blades pick up the material, spread it over heated surface in a thin film and agitate the film intensely, as it rapidly travels down. The material transforms from solution to slurry, wet cake, wet powder and finally dry powder as it travels from top to bottom. The vapour generated rises counter-currently to the inbuilt entrainment separator. Here the entrained droplets are separated from the vapour stream. The clean vapour leaves the dryer through the vapour nozzle at top.The horizontal version of the dryer is used for drying of wet cake, pastes, wet powders. The wet feed enters at one end and dry powder leaves from the opposite end. The vapours move counter currently to the powder flow and leave through vapour nozzle. | ||
==Features== | |||
* Once step drying eliminates number of steps like pre- concentration, filtration or centrifugation | * Once step drying eliminates number of steps like pre- concentration, filtration or centrifugation | ||
* Feeds can be processed without pre-concentration or dilution | * Feeds can be processed without pre-concentration or dilution | ||
| Line 23: | Line 23: | ||
* Fine powder of uniform consistency can eliminate pulverizer from downstream step | * Fine powder of uniform consistency can eliminate pulverizer from downstream step | ||
* Intense agitation suppresses fouling, keeps heat transfer surface clean | * Intense agitation suppresses fouling, keeps heat transfer surface clean | ||
* Operating pressure under vacuum, up to 1 torr* Excellent turn down capability | * Operating pressure under vacuum, up to 1 torr | ||
* Excellent turn down capability | |||
* Low product holdup, ideal for hazardous applications | * Low product holdup, ideal for hazardous applications | ||
* Different rotor configurations to suit variety of applications | * Different rotor configurations to suit variety of applications | ||
==Applications== | |||
===Drying=== | |||
* APIs, bulk drugs and intermediates | * APIs, bulk drugs and intermediates | ||
* Dyes, pigments and intermediates | * Dyes, pigments and intermediates | ||
* Organic and inorganic salts | * Organic and inorganic salts | ||
===Recoveries=== | |||
* Solvent and products from thick dry residues | * Solvent and products from thick dry residues | ||
* DMSO from salt bearing organic residues | * DMSO from salt bearing organic residues | ||
* Glycerine from salt bearing organic residues | * Glycerine from salt bearing organic residues | ||
* Water from organic and salt bearing waste water streams | * Water from organic and salt bearing waste water streams | ||
==Agitated Vacuum Dryers== | ==Agitated Vacuum Dryers== | ||
It is specially designed for drying the most delicate fine chemical products. Drying is an important part of the synthesis process and it is usually located down line of the filtration operations. The aim of this process is to remove the majority of the solvents contained in the solids. A heated agitator adds to the systems efficiency. | It is specially designed for drying the most delicate fine chemical products. Drying is an important part of the synthesis process and it is usually located down line of the filtration operations. The aim of this process is to remove the majority of the solvents contained in the solids. A heated agitator adds to the systems efficiency. | ||
==Feature== | |||
* Batch Sizes from 30 to 5,000 liters. | * Batch Sizes from 30 to 5,000 liters. | ||
* Automation for preset speed control of the main agitator | * Automation for preset speed control of the main agitator | ||
* Temperature control* Vacuum control | * Temperature control | ||
* Vacuum control | |||
* Other processes | * Other processes | ||
==Set-up== | |||
* Variable speed impeller | * Variable speed impeller | ||
* Breaker | * Breaker | ||
* Glass process vessel of 1900 ml. for 350 - 1.400 ml./batch (5 different vessel-sets available to cover 50 - 3.800 ml.) | * Glass process vessel of 1900 ml. for 350 - 1.400 ml./batch (5 different vessel-sets available to cover 50 - 3.800 ml.) | ||
* Vacuum system; dust filter, glass condenser, bypass, vacuum pump, process pressure control | * Vacuum system; dust filter, glass condenser, bypass, vacuum pump, process pressure control | ||
* Nitrogen purge* The system can be build on a frame to be incorporated in a hood | * Nitrogen purge | ||
* The system can be build on a frame to be incorporated in a hood | |||
* Critical process data: impeller torque, product temperature, impeller speed, process pressure, mass recovered liquid, process vessel/condenser/filter jacket temperature, mass recovered liquid, RH (optional), vapour temp (optional) | * Critical process data: impeller torque, product temperature, impeller speed, process pressure, mass recovered liquid, process vessel/condenser/filter jacket temperature, mass recovered liquid, RH (optional), vapour temp (optional) | ||
* PC/PLC automation package: "real-time"-trending and batch reporting in Excel of all critical process data and batch identification | * PC/PLC automation package: "real-time"-trending and batch reporting in Excel of all critical process data and batch identification | ||
==Options== | |||
* Chopper for de-lumping | * Chopper for de-lumping | ||
* 21CFRPart11 compliant software | * 21CFRPart11 compliant software | ||
* RH control in process vessel, vapour Temp | * RH control in process vessel, vapour Temp | ||
* Trolley | * Trolley GAS assisted drying | ||
* Hastelloy C22 product contact parts | * Hastelloy C22 product contact parts | ||
* Cooling & heating unit | * Cooling & heating unit | ||
| Line 63: | Line 78: | ||
* Validation IQ/OQ/SQ | * Validation IQ/OQ/SQ | ||
* Integration in Containment isolator (Stainless Steel, Polycarbonate, PE,..) | * Integration in Containment isolator (Stainless Steel, Polycarbonate, PE,..) | ||
==Video== | ==Video== | ||
<youtube>LQnhtk9WrLA</youtube> | <youtube>LQnhtk9WrLA</youtube> | ||
Latest revision as of 04:57, 20 February 2013
The Agitated Dryers are presently used widely over the chemical Industry. These are naturally of 2 different types. These are:
- Agitated Thin Film Dryers
- Agitated Vacuum Dryers
Agitated Thin Film Dryers
Mechanically Agitated Thin Film Dryer is an indirectly heated continuous dryer. The feed can be in the form of a solution, slurry, wet cake or paste. If required it operates under vacuum. We offer both vertical and horizontal versions. Mechanically Agitated Thin Film Dryer is an indirectly heated continuous dryer. The feed can be in the form of a solution, slurry, wet cake or paste. If required it operates under vacuum. We offer both vertical and horizontal versions.
Working Principle
The drying in a agitated thin film dryer is a continuous operation under vacuum. Operating pressures can be as low as 1 mbar and operating temperatures can be as high as 350oC. Drying time depends on material being dried, amount of solvent to be removed, desired final moisture content, permissible jacket temperature etc.The vertical Agitated Thin Film Dryer has a jacketed cylinder with a closely fitting rotor at the centre. During operation the rotor revolves at high speed. The feed distributor spreads the incoming feed uniformly over the cylinder top periphery. The rotor blades pick up the material, spread it over heated surface in a thin film and agitate the film intensely, as it rapidly travels down. The material transforms from solution to slurry, wet cake, wet powder and finally dry powder as it travels from top to bottom. The vapour generated rises counter-currently to the inbuilt entrainment separator. Here the entrained droplets are separated from the vapour stream. The clean vapour leaves the dryer through the vapour nozzle at top.The horizontal version of the dryer is used for drying of wet cake, pastes, wet powders. The wet feed enters at one end and dry powder leaves from the opposite end. The vapours move counter currently to the powder flow and leave through vapour nozzle.
Features
- Once step drying eliminates number of steps like pre- concentration, filtration or centrifugation
- Feeds can be processed without pre-concentration or dilution
- Indirect heating and drying in absence of air. Particularly effective for heat, light and oxygen sensitive products. Best suited for solvent bearing products for complete solvent recovery
- Quick processing time, best suitable for heat sensitive products
- Probably the most energy efficient dryer in the market. Thermal efficiency exceeds 90%
- Fine powder of uniform consistency can eliminate pulverizer from downstream step
- Intense agitation suppresses fouling, keeps heat transfer surface clean
- Operating pressure under vacuum, up to 1 torr
- Excellent turn down capability
- Low product holdup, ideal for hazardous applications
- Different rotor configurations to suit variety of applications
Applications
Drying
- APIs, bulk drugs and intermediates
- Dyes, pigments and intermediates
- Organic and inorganic salts
Recoveries
- Solvent and products from thick dry residues
- DMSO from salt bearing organic residues
- Glycerine from salt bearing organic residues
- Water from organic and salt bearing waste water streams
Agitated Vacuum Dryers
It is specially designed for drying the most delicate fine chemical products. Drying is an important part of the synthesis process and it is usually located down line of the filtration operations. The aim of this process is to remove the majority of the solvents contained in the solids. A heated agitator adds to the systems efficiency.
Feature
- Batch Sizes from 30 to 5,000 liters.
- Automation for preset speed control of the main agitator
- Temperature control
- Vacuum control
- Other processes
Set-up
- Variable speed impeller
- Breaker
- Glass process vessel of 1900 ml. for 350 - 1.400 ml./batch (5 different vessel-sets available to cover 50 - 3.800 ml.)
- Vacuum system; dust filter, glass condenser, bypass, vacuum pump, process pressure control
- Nitrogen purge
- The system can be build on a frame to be incorporated in a hood
- Critical process data: impeller torque, product temperature, impeller speed, process pressure, mass recovered liquid, process vessel/condenser/filter jacket temperature, mass recovered liquid, RH (optional), vapour temp (optional)
- PC/PLC automation package: "real-time"-trending and batch reporting in Excel of all critical process data and batch identification
Options
- Chopper for de-lumping
- 21CFRPart11 compliant software
- RH control in process vessel, vapour Temp
- Trolley GAS assisted drying
- Hastelloy C22 product contact parts
- Cooling & heating unit
- NIR or MIR probe integration
- Different vessel-sets to cover 50 - 3800 ml
- Combined unit with Nutsche Filter Dryer
- Validation IQ/OQ/SQ
- Integration in Containment isolator (Stainless Steel, Polycarbonate, PE,..)
Video